anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

Base Information

Chemical Name:anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]
CAS No.:268728-63-8
Molecular Formula:C₆₀H₄₄N₄O₂
Molecular Weight:853.035
Hs Code.:

Synonyms:anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

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Chemical Property of anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

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Technology Process of anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

There total 2 articles about anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 159152-14-4
5-(mesityl)dipyrromethane

: 82-86-0
acenaphthene quinone

: 268728-63-8
anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

: 268728-62-7
C₆₀H₄₄N₄O₂

Guidance literature:: 5-(mesityl)dipyrromethane; acenaphthene quinone; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 4h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/a907992k

Reference yield: 15.0%

: 159152-14-4
5-(mesityl)dipyrromethane

: 82-86-0
acenaphthene quinone

: syn-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

: 268728-63-8
anti-dispiro[2H-acenaphthylen-1-one-2,5'-10',20'-dimesityldihydroporphyrin-15',2'',2''H-acenaphthylen-1''-one]

Guidance literature:: 5-(mesityl)dipyrromethane; acenaphthene quinone; With boron trifluoride diethyl etherate; In dichloromethane; for 3h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1h; Further stages.;
DOI:10.1021/jo010163l