Technology Process of 4-(4'-O-acetylphenyl)-3-cyano-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone
There total 1 articles about 4-(4'-O-acetylphenyl)-3-cyano-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H22O8; cyanoacetic acid amide;
With
potassium tert-butylate;
In
dimethyl sulfoxide;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
oxygen;
In
dimethyl sulfoxide;
acetic anhydride;
With
pyridine;
In
dimethyl sulfoxide;
at 0 ℃;
DOI:10.1016/j.carres.2011.03.006
- Guidance literature:
-
4-(4'-O-acetylphenyl)-3-cyano-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone;
With
sodium methylate;
In
methanol;
at 25 ℃;
With
hydrogenchloride;
In
methanol; water;
at 0 ℃;
DOI:10.1016/j.carres.2011.03.006
