2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

Base Information

Chemical Name:2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide
CAS No.:97150-67-9
Molecular Formula:C₁₄H₁₁N₅O₂
Molecular Weight:281.274
Hs Code.:

Synonyms:2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

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Chemical Property of 2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

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Technology Process of 2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

There total 5 articles about 2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97150-66-8
2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxylic acid hydrazine

: 97150-67-9
2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 22.7 g / 12N aq. HCl / 18 h / Heating

2: 11.6 g / SOCl₂, Et₃N, NH₃ / dimethylformamide

With hydrogenchloride; thionyl chloride; ammonia; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00148a006

Reference yield:

: 97150-68-0
2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxylic acid hydrochloride

: 97150-67-9
2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

Guidance literature:: With thionyl chloride; ammonia; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00148a006

Reference yield:

: 97150-79-3
hydroxy<2-<4-(1H-imidazol-1-yl)phenyl>-2-oxoethyl>propanedioic acid diethyl ester

: 97150-67-9
2,3-dihydro-6-<4-(1H-imidazol-1-yl)phenyl>-3-oxo-4-pyridazinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80.2 g / hydrazine hydrate / methanol / 18 h / Heating

2: 22.7 g / 12N aq. HCl / 18 h / Heating

3: 11.6 g / SOCl₂, Et₃N, NH₃ / dimethylformamide

With hydrogenchloride; thionyl chloride; ammonia; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00148a006