α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol

Base Information

• Chemical Name: α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol
• CAS No.: 70875-80-8
• Molecular Formula: C₂₀H₂₇NO₂S
• Molecular Weight: 345.506

Synonyms:α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol

Chemical Property of α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol

Chemical Property:

Purity/Quality:

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Technology Process of α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol

There total 2 articles about α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid 4-[2-(1,1-dimethyl-3-phenyl-propylamino)-acetyl]-2-methylsulfanyl-phenyl ester → α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol (70875-80-8)

Guidance literature:

Multistep reaction; (i) NaBH₄, MeOH, (ii) KOH;

Reference yield:

1,1-Dimethyl-3-phenyl-propylamin (43052-72-8) + 2-bromo-4'-hydroxy-3'-(methylthio)acetophenone 4'-acetate (66264-58-2) → α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol (70875-80-8)

Guidance literature:

Multi-step reaction with 2 steps

2: (i) NaBH₄, MeOH, (ii) KOH

Reference yield:

α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzenemethanol (70875-80-8) → α-{[(1,1-dimethyl-3-phenylpropyl)amino]methyl}-4-hydroxy-3-(methylthio)benzyl chloride hydrochloride

Guidance literature:

With thionyl chloride;

upstream raw materials:

1,1-Dimethyl-3-phenyl-propylamin

2-bromo-4'-hydroxy-3'-(methylthio)acetophenone 4'-acetate

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