(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

Base Information

Chemical Name:(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]
CAS No.:1092408-84-8
Molecular Formula:C₂₉H₂₆ClFN₂O₄
Molecular Weight:520.988
Hs Code.:

Synonyms:(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

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Chemical Property of (R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

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Technology Process of (R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

There total 1 articles about (R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 813426-25-4
RWJ-676070

: 1092408-84-8
(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

Guidance literature:: RWJ-676070; With sodium azide; sulfuric acid; In chloroform; at 50 ℃; for 3.33333h;

With sodium hydroxide; water; at 0 ℃; for 0.333333h;

Reference yield:

: 1092408-84-8
(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

: 1092408-47-3
(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-hydroxyimino-spiro[cyclopentane-1,4'-benzo[b]azepane]

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 1h;

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1092408-84-8
(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]

: 1092408-87-1
C₃₃H₃₂ClFN₂O₅

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(R)-N-[3-methoxy-4-(2-chloro-5-fluoro-phenylcarbonyl)amino-phenylcarbonyl]-3-oxo-spiro[cyclopentane-1,4'-benzo[b]azepane]; In tetrahydrofuran; at 20 ℃; for 16.0833h;