Technology Process of 3-allyloxy-4,5-dimethoxytoluene
There total 5 articles about 3-allyloxy-4,5-dimethoxytoluene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 15h;
Heating;
DOI:10.1055/s-1993-25945
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating
2: 93 percent / K2CO3 / Bu4NHSO4 / acetone / 24 h / Heating
3: TsOH / methanol; H2O / 16 h / Ambient temperature
4: 90 percent / K2CO3 / acetone / 15 h / Heating
With
4 A molecular sieve; potassium carbonate; toluene-4-sulfonic acid;
Amberlite IR 120-plus; tetra(n-butyl)ammonium hydrogensulfate;
In
methanol; water; acetone; benzene;
DOI:10.1055/s-1993-25945
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 97 percent / H2 / 10percent Pd/C / acetic acid / 72 h / 30002.4 Torr / Ambient temperature
2: 96 percent / 57percent HI, 30percent aq. H3PO2 / Heating
3: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating
4: 93 percent / K2CO3 / Bu4NHSO4 / acetone / 24 h / Heating
5: TsOH / methanol; H2O / 16 h / Ambient temperature
6: 90 percent / K2CO3 / acetone / 15 h / Heating
With
4 A molecular sieve; hydrogen iodide; hydrogen; hypophosphorous acid; potassium carbonate; toluene-4-sulfonic acid;
palladium on activated charcoal; Amberlite IR 120-plus; tetra(n-butyl)ammonium hydrogensulfate;
In
methanol; water; acetic acid; acetone; benzene;
DOI:10.1055/s-1993-25945
