trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Base Information

• Chemical Name: trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole
• CAS No.: 73327-06-7
• Molecular Formula: C₁₉H₂₄N₂O₂
• Molecular Weight: 312.412

Synonyms:trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Chemical Property of trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

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Technology Process of trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

There total 12 articles about trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-benzyl-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-cyclohexane (73327-01-2) → trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole (73327-06-7)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol;

DOI:10.1021/jo951170a

Reference yield: 10.0%

→ cis-(3-(methoxycarbonyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-yl)cyclohexane (75140-08-8) + trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole (73327-06-7)

Guidance literature:

With sodium cyanoborohydride; In methanol; at -70 - -20 ℃;

Reference yield: 10.0%

1-cyclohexyl-3-methoxycarbonyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide (104330-96-3) → cis-(3-(methoxycarbonyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-yl)cyclohexane (75140-08-8) + trans-1-cyclohexyl-3-(methoxycarbonyl)-1-propyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole (73327-06-7)

Guidance literature:

With sodium cyanoborohydride; In methanol; at -78 ℃; for 1h;

DOI:10.1248/cpb.33.3237

upstream raw materials:

2-benzyl-3-(methoxycarbonyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-cyclohexane

trans-1-cyclohexyl-3-(methoxycarbonyl)-2-(diphenylmethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

1-cyclohexyl-3-methoxycarbonyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

DL-tryptophan methyl ester

Downstream raw materials:

trans-(3-(hydroxymethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-yl)cyclohexane

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