N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

Base Information

Chemical Name:N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide
CAS No.:1313816-39-5
Molecular Formula:C₄₂H₄₄N₂O₄S
Molecular Weight:672.888
Hs Code.:

Synonyms:N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

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Chemical Property of N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

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Technology Process of N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

There total 6 articles about N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1313816-36-2
((4aR,7S,7aR,12bS)-3-(3-(3-tritylthio)propanamido)butyl)-2,3,4,4a,7,7a-hexahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinoline-7,9-diyl diacetate

: 1313816-39-5
N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

Guidance literature:: With water; sodium hydroxide; In methanol; at 20 ℃; for 0.75h;
DOI:10.1021/jm200461m

Reference yield:

: 1313816-26-0
(4aR,7S,7aR,12bS)-3-(3-((tert-butoxycarbonyl)amino)butyl)-2,3,4,4a,7,7a-hexahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinoline-7,9-diyl diacetate

: 1313816-39-5
N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 2 h / 20 °C

2: triethylamine / dichloromethane / 2 h / 0 °C

3: water; sodium hydroxide / methanol / 0.75 h / 20 °C

With water; triethylamine; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/jm200461m

Reference yield:

: 1313816-31-7
C₂HF₃O₂*C₂₄H₃₀N₂O₅

: 1313816-39-5
N-(3-(4aR,7S,7aR,12bS)-7,9-dihydroxy-4,4a,7,7a-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-3(2H)-yl)butyl-3-(tritylthio)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 °C

2: water; sodium hydroxide / methanol / 0.75 h / 20 °C

With water; triethylamine; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/jm200461m