4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile

Base Information

• Chemical Name: 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile
• CAS No.: 31186-79-5
• Molecular Formula: C₁₈H₁₂Cl₂N₂O₃
• Molecular Weight: 375.211

Synonyms:4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile

Chemical Property of 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile

Chemical Property:

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Technology Process of 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile

There total 4 articles about 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

E-1-(4'-methoxyphenyl)prop-1-ene (4180-23-8,25086-72-0,63589-56-0) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → 4-methoxy-trans-cinnamaldehyde (24680-50-0,71277-11-7,1963-36-6) + 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (31186-79-5) + 4,5-Dichloro-3,6-bis-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (33904-07-3)

Guidance literature:

DOI:10.3891/acta.chem.scand.52-1177

Reference yield:

Estragole (140-67-0) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → 4-methoxycinnamaldehyde (1963-36-6) + 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (31186-79-5) + 4,5-Dichloro-3,6-bis-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (33904-07-3)

Guidance literature:

In dichloromethane; water; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4039(98)00213-5

Reference yield:

2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) + anethole (104-46-1,25086-72-0,63589-56-0) → 4-methoxycinnamaldehyde (1963-36-6) + 4,5-Dichloro-3-hydroxy-6-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (31186-79-5) + 4,5-Dichloro-3,6-bis-[(E)-3-(4-methoxy-phenyl)-allyloxy]-phthalonitrile (33904-07-3)

Guidance literature:

In dichloromethane; water; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4039(98)00213-5

upstream raw materials:

Estragole

2,3-dicyano-5,6-dichloro-p-benzoquinone

anethole

E-1-(4'-methoxyphenyl)prop-1-ene

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