Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2]

Base Information

• Chemical Name: Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2]
• CAS No.: 79969-12-3
• Molecular Formula: C₂Cl₂O₂Rh*C₂₀H₂₀N₂O₂Rh
• Molecular Weight: 653.129

Synonyms:Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2]

Chemical Property of Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2]

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Technology Process of Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2]

There total 1 articles about Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)⁽¹⁺⁾*RhCl₂(CO)2^(1-)=[Rh(CO)2((CH₃)2C₆H₃NCHCHNC₆H₃(CH₃)2)][RhCl₂(CO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(rhodium)tetracarbonyl dichloride + glyoxalbis(2,6-dimethylphenylimine) → Rh(CO)2((CH3)2C6H3NCHCHNC6H3(CH3)2)(1+)*RhCl2(CO)2(1-)=[Rh(CO)2((CH3)2C6H3NCHCHNC6H3(CH3)2)][RhCl2(CO)2] (79969-12-3)

Guidance literature:

In hexane; N2-atmosphere; addn. of ligand to Rh-complex, stirring (5 min, pptn.); collection (filtration), washing (hexane), drying (vac., room temp.); elem. anal.;

DOI:10.1016/S0020-1693(00)88345-0

Reference yield:

Rh(CO)2((CH3)2C6H3NCHCHNC6H3(CH3)2)(1+)*RhCl2(CO)2(1-)=[Rh(CO)2((CH3)2C6H3NCHCHNC6H3(CH3)2)][RhCl2(CO)2] (79969-12-3) → chlorocarbonylbis(triphenylphosphine)rhodium(I) (15318-33-9,16353-77-8,13938-94-8)

Guidance literature:

With triphenylphosphine; In dichloromethane; byproducts: CO; N2-atmosphere; molar ratio Rh:PPh3=1:1.5, addn. of PPh3 to Rh-complex, stirring (15 min); solvent removal (reduced pressure), washing (hexane), drying (vac., roomtemp.);

DOI:10.1016/S0020-1693(00)88345-0

Downstream raw materials:

chlorocarbonylbis(triphenylphosphine)rhodium(I)

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