2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

Base Information

Chemical Name:2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine
CAS No.:1247712-58-8
Molecular Formula:C₁₇H₁₃Cl₄N₃O
Molecular Weight:417.122
Hs Code.:

Synonyms:2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

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Chemical Property of 2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

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Technology Process of 2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

There total 4 articles about 2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1247712-54-4
3-[(benzyloxy)methyl]-1-(3-chloropyridin-2-yl)-5-(trichloromethyl)-4,5-dihydro-1H-pyrazol-5-ol

: 1247712-58-8
2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

Guidance literature:: With trifluoroacetic anhydride; In isobutyl methyl ether; at 25 ℃; for 2h;

Reference yield: 95.0%

: 1247712-58-8
2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

Guidance literature:

Reference yield:

: 4039-82-1
Benzyl propargyl ether

: 1247712-58-8
2-{3-[(benzyloxy)methyl]-5-(trichloromethyl)-1H-pyrazol-1-yl}-3-chloropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium

2: tert-butyl methyl ether / 1 h / 30 °C

3: trifluoroacetic anhydride / isobutyl methyl ether / 2 h / 25 °C

With n-butyllithium; trifluoroacetic anhydride; In tert-butyl methyl ether; isobutyl methyl ether;