3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

Base Information

Chemical Name:3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride
CAS No.:887914-50-3
Molecular Formula:C₄₁H₇₁ClO₃
Molecular Weight:647.466
Hs Code.:

Synonyms:3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

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Chemical Property of 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

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Technology Process of 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

There total 11 articles about 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 887914-49-0
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl alcohol

: 887914-50-3
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja0606935

Reference yield:

: 7766-49-6
1-iodo-10-undecene

: 887914-50-3
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / K₂CO₃ / dimethylformamide / 3 h / 70 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 3 h / 20 °C

3: 92 percent / SOCl₂ / CH₂Cl₂ / 4 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0606935

Reference yield:

: 887914-38-7
ethyl 3,5-bis[(tert-butyldimethylsilyl)oxy]-4-hydroxybenzoate

: 887914-50-3
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 10 h / 20 °C

2: 100 percent / tetrabutylammonium fluoride / CH₂Cl₂ / 10 h / 20 °C

3: 78 percent / K₂CO₃ / dimethylformamide / 3 h / 70 °C

4: 94 percent / LiAlH₄ / tetrahydrofuran / 3 h / 20 °C

5: 92 percent / SOCl₂ / CH₂Cl₂ / 4 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; tetrabutyl ammonium fluoride; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1021/ja0606935