N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Base Information

Chemical Name:N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide
CAS No.:917881-54-0
Molecular Formula:C₂₂H₁₆N₂O₃S
Molecular Weight:388.447
Hs Code.:

Synonyms:N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Suppliers and Price of N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

There total 7 articles about N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: N-(2,4-dimethoxybenzyl)-N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

: 917881-54-0
N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jm200112k

Reference yield:

: 7-[(2,4-dimethoxybenzyl)amino]-3-phenyl-5H-5Hbenzo[4,5]cyclohepta[1,2-b]pyridin-5-one

: 917881-54-0
N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 0.08 h / Inert atmosphere

With 4-methyl-morpholine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm200112k

Reference yield:

: 612822-21-6
7-bromo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one

: 917881-54-0
N-(5-oxo-3-phenyl-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-7-yl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / 1,4-dioxane / 100 °C / Inert atmosphere

2: 4-methyl-morpholine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 0.08 h / Inert atmosphere

With 4-methyl-morpholine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid; sodium t-butanolate; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm200112k