Technology Process of C22H33N5O6
There total 1 articles about C22H33N5O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: methanol / 0.25 h
2.1: water; lithium hydroxide / tetrahydrofuran / 2.5 h
3.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
3.2: 15 h
4.1: zinc; acetic acid / water / 0.5 h
5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / -78 - 20 °C
6.1: hydrogenchloride / ethyl acetate / 3.5 h / 0 °C
7.1: sodium hydrogencarbonate / dichloromethane
8.1: ammonium formate / palladium 10% on activated carbon / isopropyl alcohol / 0.13 h / 85 °C / microwave irradiation
With
hydrogenchloride; water; ammonium formate; sodium hydrogencarbonate; benzotriazol-1-ol; O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; zinc;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; isopropyl alcohol;
- Guidance literature:
-
With
benzotriazol-1-ol; O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
