C₆₀H₇₂I₂O₄

Base Information

Chemical Name:C₆₀H₇₂I₂O₄
CAS No.:1267662-17-8
Molecular Formula:C₆₀H₇₂I₂O₄
Molecular Weight:1111.04
Hs Code.:

C<sub>60</sub>H<sub>72</sub>I<sub>2</sub>O<sub>4</sub>

Synonyms:C₆₀H₇₂I₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₀H₇₂I₂O₄

Chemical Property:

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Technology Process of C₆₀H₇₂I₂O₄

There total 8 articles about C₆₀H₇₂I₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1267662-16-7
C₆₆H₉₀O₄Si₂

: 1267662-17-8
C₆₀H₇₂I₂O₄

Guidance literature:: With Iodine monochloride; In dichloromethane; at 0 ℃; for 12.5h; Inert atmosphere;
DOI:10.1002/chem.201002574

Reference yield:

: 111-25-1
1-bromo-hexane

: 1267662-17-8
C₆₀H₇₂I₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / butanone / 24 h / Inert atmosphere; Reflux

2.1: n-butyllithium / diethyl ether; hexane / 1.17 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 48 h / 80 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

5.1: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

7.1: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium acetate; Iodine monochloride; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; butanone;
DOI:10.1002/chem.201002574

Reference yield:

: 517895-16-8
1,3-dibromo-5-(hexyloxy)benzene

: 1267662-17-8
C₆₀H₇₂I₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / diethyl ether; hexane / 1.17 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 48 h / 80 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

4.1: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

6.1: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium acetate; Iodine monochloride; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201002574