2,4-Dimethyl-3-β-hydroxyethylanisole

Base Information

• Chemical Name: 2,4-Dimethyl-3-β-hydroxyethylanisole
• CAS No.: 33348-63-9
• Molecular Formula: C₁₁H₁₆O₂
• Molecular Weight: 180.247

Synonyms:2,4-Dimethyl-3-β-hydroxyethylanisole

Chemical Property of 2,4-Dimethyl-3-β-hydroxyethylanisole

Chemical Property:

Purity/Quality:

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Technology Process of 2,4-Dimethyl-3-β-hydroxyethylanisole

There total 3 articles about 2,4-Dimethyl-3-β-hydroxyethylanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl 2,6-dimethyl-3-methoxy-1-phenylacetate (118304-33-9) → 2,4-Dimethyl-3-β-hydroxyethylanisole (33348-63-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; 1) 12 h, RT 2) 4-5 h, reflux;

Reference yield:

8-methoxy-5-methyl-isochroman (33348-62-8) → 2,4-Dimethyl-3-β-hydroxyethylanisole (33348-63-9)

Guidance literature:

With ammonia; lithium; In 1,2-dimethoxyethane; at -33 ℃;

DOI:10.1016/S0040-4020(01)98049-4

Reference yield:

→ 2,4-Dimethyl-3-β-hydroxyethylanisole (33348-63-9)

Guidance literature:

2,6-Dimethyl-3-methoxyphenylessigsaeure, 1. Diazomethan, 2. LiAlH4;

DOI:10.1021/ja01482a036

upstream raw materials:

methyl 2,6-dimethyl-3-methoxy-1-phenylacetate

8-methoxy-5-methyl-isochroman

Downstream raw materials:

2,4-Dimethyl-3-β-methoxyethylanisole

2,6-Dimethyl-3-methoxy-phenylessigsaeure

2-Methoxy-4-β-methoxyethyl-2',3,5-trimethylcinnamic acid

2-Methoxy-4-β-methoxyethyl-2',3,5-trimethyldihydrocinnamic acid

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