N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline

Base Information

• Chemical Name: N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline
• CAS No.: 1393736-07-6
• Molecular Formula: C₂₄H₁₉N₅O₅S
• Molecular Weight: 489.511

Synonyms:N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline

Chemical Property of N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline

Chemical Property:

Purity/Quality:

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Technology Process of N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline

There total 3 articles about N₁-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-4-chloro-N2-(4'-cyanophenyl)-5-aminosulfonyl-nitrobenzene (1393735-99-3) → N1-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline (1393736-07-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 130 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 3 h / 20 °C

With potassium tert-butylate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jm3007678

Reference yield:

2,4-dichloronitrobenzene (611-06-3) → N1-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline (1393736-07-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: chlorosulfonic acid / 0 - 140 °C

2.1: ammonium hydroxide / tetrahydrofuran / 0 °C

3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0 - 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 130 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

5.2: 3 h / 20 °C

With chlorosulfonic acid; ammonium hydroxide; potassium tert-butylate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jm3007678

Reference yield:

2,4-dichloro-5-nitrobenzenesulfonamide (4818-74-0) → N1-(4'-cyanophenyl)-5-(4''-(2-cyanovinyl)-2'',6''-dimethylphenoxy)-4-sulfamoyl-2-nitroaniline (1393736-07-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium tert-butylate / N,N-dimethyl-formamide / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 130 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 3 h / 20 °C

With potassium tert-butylate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jm3007678

upstream raw materials:

2-amino-4-chloro-N₂-(4'-cyanophenyl)-5-aminosulfonyl-nitrobenzene

2,4-dichloronitrobenzene

2,4-dichloro-5-nitrobenzenesulfonamide

Downstream raw materials:

5-(4''-cyanoethyl-2'',6''-dimethylphenoxy)-N₁-(4'-cyanophenyl)-4-aminosulfonyl-1,2-phenylenediamine

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