C₄₅H₅₆N₈O₆S₂

Base Information

Chemical Name:C₄₅H₅₆N₈O₆S₂
CAS No.:1419385-55-9
Molecular Formula:C₄₅H₅₆N₈O₆S₂
Molecular Weight:869.122
Hs Code.:

C<sub>45</sub>H<sub>56</sub>N<sub>8</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₄₅H₅₆N₈O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₅₆N₈O₆S₂

Chemical Property:

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Technology Process of C₄₅H₅₆N₈O₆S₂

There total 15 articles about C₄₅H₅₆N₈O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.2%

: C₃₁H₃₄N₆S₂*4ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1419385-55-9
C₄₅H₅₆N₈O₆S₂

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h; Cooling with ice;

Reference yield: 50.2%

: C₃₁H₃₄N₆S₂

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1419385-55-9
C₄₅H₅₆N₈O₆S₂

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h; Cooling with ice;

Reference yield:

: 1419387-60-2
C₁₅H₁₈O₂

: 1419385-55-9
C₄₅H₅₆N₈O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

3.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

3.2: 4 h / 0 °C

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 12 h / 20 °C / Cooling with ice

5.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 6 h / 140 °C / Sealed tube

6.1: dichloromethane; ethyl acetate / 12 h / 20 °C

7.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C / Cooling with ice

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; ammonium acetate; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; ethyl acetate; acetonitrile;