trans-β-styrylamine-N,N-disiliciee nitrile

Base Information

• Chemical Name: trans-β-styrylamine-N,N-disiliciee nitrile
• CAS No.: 78108-67-5
• Molecular Formula: C₁₈H₂₃NSi₂
• Molecular Weight: 309.558
• Mol file: 78108-67-5.mol

Synonyms:trans-β-styrylamine-N,N-disiliciee nitrile

Chemical Property of trans-β-styrylamine-N,N-disiliciee nitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-β-styrylamine-N,N-disiliciee nitrile

There total 2 articles about trans-β-styrylamine-N,N-disiliciee nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,2-bis(dimethylsilyl)benzene (17985-72-7) + phenylacetonitrile (140-29-4) → trans-β-styrylamine-N,N-disiliciee nitrile (78108-67-5)

Guidance literature:

With Wilkinson's catalyst; In toluene; for 60h; Heating;

DOI:10.1016/S0022-328X(00)84331-4

Reference yield:

phenylacetonitrile (140-29-4) → trans-β-styrylamine-N,N-disiliciee nitrile (78108-67-5) + C18H23NSi2 (78108-68-6)

Guidance literature:

In hexane; for 21h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature; Irradiation;

DOI:10.1021/jo00329a057

Reference yield: 79.0%

trans-β-styrylamine-N,N-disiliciee nitrile (78108-67-5) → phenylacetaldehyde (122-78-1)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/jo00329a057

upstream raw materials:

1,2-bis(dimethylsilyl)benzene

phenylacetonitrile

Downstream raw materials:

phenylacetaldehyde

benzaldehyde

1,4-diphenyl-2-aza-1,3-butadiene