Bis(4-Nitrophenyl) phosphorazidate

Base Information

• Chemical Name: Bis(4-Nitrophenyl) phosphorazidate
• CAS No.: 51250-91-0
• Molecular Formula: C12H8 N5 O7 P
• Molecular Weight: 365.19
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID70454071
• Nikkaji Number: J2.194.027E
• Wikidata: Q72499258
• Mol file: 51250-91-0.mol

Synonyms:51250-91-0;Bis(4-Nitrophenyl) phosphorazidate;Bis(p-nitrophenyl) Azidophosphonate;Bis(p-nitrophenyl)azidophosphonate;Bis(4-Nitrophenyl)phosphorazidate;1-[azido-(4-nitrophenoxy)phosphoryl]oxy-4-nitrobenzene;Phosphorazidic acid, bis(4-nitrophenyl) ester;SCHEMBL5246734;DTXSID70454071;BCA25091;BCP19650;Bis (4-nitrophenyl) azidophosphonate;MFCD08274943;AKOS016005109;s11922;AS-20023;FT-0688589;Azidophosphoric acid bis(4-nitrophenyl) ester

Chemical Property of Bis(4-Nitrophenyl) phosphorazidate

Chemical Property:

• PSA: 186.73000
• LogP: 4.87836
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 9
• Rotatable Bond Count: 5
• Exact Mass: 365.01613461
• Heavy Atom Count: 25
• Complexity: 544

Purity/Quality:

97% ^*data from raw suppliers

BIS-(PARA-NITROPHENYL)AZIDOPHOSPHONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1[N+](=O)[O-])OP(=O)(N=[N+]=[N-])OC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of Bis(4-Nitrophenyl) phosphorazidate

There total 1 articles about Bis(4-Nitrophenyl) phosphorazidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

diphenyl phosphoryl azide (26386-88-9) → bis(p-nitrophenyl) azidophosphonate (51250-91-0)

Guidance literature:

With nitric acid; at 0 ℃; for 0.5h;

DOI:10.1016/j.tet.2022.132642

Reference yield: 94.0%

bis(p-nitrophenyl) azidophosphonate (51250-91-0) + 2,3,4,6-tetra-O-benzyl-D-galactopyranose (6386-24-9) + 1,8-diazabicyclo[5.4.0]undec-7-ene (6674-22-2,83329-50-4) → 2,3,4,6-tetra-O-benzyl-D-galactopyranosyl azide

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield: 84.0%

bis(p-nitrophenyl) azidophosphonate (51250-91-0) + methyl 5-hydroxy-3-cyclohexenecarboxylate (79433-96-8) + 1,8-diazabicyclo[5.4.0]undec-7-ene (6674-22-2,83329-50-4) → (E)-3-azido-5-methoxycarbonyl-1-cyclohexene

Guidance literature:

In tetrahydrofuran;

upstream raw materials:

diphenyl phosphoryl azide

Downstream raw materials:

[1-Phenyl-1-pyrrolidin-1-yl-meth-(Z)-ylidene]-phosphoramidic acid bis-(4-nitro-phenyl) ester

[2-Phenyl-2-pyridin-2-yl-1-pyrrolidin-1-yl-eth-(Z)-ylidene]-phosphoramidic acid bis-(4-nitro-phenyl) ester

phenyldiazomethane

[1-Pyridin-2-yl-1-pyrrolidin-1-yl-meth-(Z)-ylidene]-phosphoramidic acid bis-(4-nitro-phenyl) ester

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