C₃₁H₅₃ISi

Base Information

• Chemical Name: C₃₁H₅₃ISi
• CAS No.: 952054-12-5
• Molecular Formula: C₃₁H₅₃ISi
• Molecular Weight: 580.752
• Mol file: 952054-12-5.mol

Synonyms:C₃₁H₅₃ISi

Chemical Property of C₃₁H₅₃ISi

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₃₁H₅₃ISi

There total 1 articles about C₃₁H₅₃ISi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4,5-didecyl-1,2-diiodobenzene (191231-92-2) + trimethylsilylacetylene (1066-54-2) → C31H53ISi (952054-12-5)

Guidance literature:

With copper(l) iodide; diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 80 ℃; for 3h;

DOI:10.1021/ol7014253

Reference yield: 94.0%

C31H53ISi (952054-12-5) + prop-1-yne (74-99-7) → C34H56Si (952054-13-6)

Guidance literature:

With copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 40 - 50 ℃;

DOI:10.1021/ol7014253

Reference yield: 84.0%

C31H53ISi (952054-12-5) + tris-iso-propylsilyl acetylene (89343-06-6) → C42H74Si2 (1242773-47-2)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In tetrahydrofuran; at 50 ℃; Inert atmosphere;

DOI:10.1021/ol101542e

upstream raw materials:

4,5-didecyl-1,2-diiodobenzene

trimethylsilylacetylene

Downstream raw materials:

C₃₄H₅₆Si

C₄₂H₇₄Si₂