N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

Base Information

Chemical Name:N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff
CAS No.:128540-96-5
Molecular Formula:C₁₈H₁₃ClF₃N₃O₄S
Molecular Weight:459.833
Hs Code.:

Synonyms:N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

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Technology Process of N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

There total 3 articles about N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 128540-89-6
5-Aminomethyl-2-phenyl-4-trifluoromethyloxazole

: 5769-15-3
4-Chlorophenylsulfonyl isocyanate

: 128540-96-5
N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

Guidance literature:: In toluene; at 90 ℃; for 3h;
DOI:10.1055/s-1990-26878

Reference yield:

: 70276-69-6
5-Fluoro-4-trifluoromethyl-2-phenyloxazole

: 128540-96-5
N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / dibenzo-18-crown-6 / acetonitrile / Heating

2: 48 percent / LiAlH₄ / diethyl ether / 16 h / Ambient temperature

3: 70 percent / toluene / 3 h / 90 °C

With lithium aluminium tetrahydride; dibenzo-18-crown-6; In diethyl ether; toluene; acetonitrile;
DOI:10.1055/s-1990-26878

Reference yield:

: 122884-78-0
5-Cyano-2-phenyl-4-trifluoromethyloxazole

: 128540-96-5
N-<(2-Phenyl-4-trifluormethyloxazol-5-yl)-methyl>-N'-(4-chlorbenzosulfonyl)-harnstoff

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / LiAlH₄ / diethyl ether / 16 h / Ambient temperature

2: 70 percent / toluene / 3 h / 90 °C

With lithium aluminium tetrahydride; In diethyl ether; toluene;
DOI:10.1055/s-1990-26878