ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

Base Information

Chemical Name:ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate
CAS No.:1207984-53-9
Molecular Formula:C₁₉H₃₀N₂O₂
Molecular Weight:318.459
Hs Code.:

Synonyms:ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

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Chemical Property of ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

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Technology Process of ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

There total 7 articles about ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1207984-52-8
ethyl 7-[(5-cyclopropyl-4-methyl-2-nitrophenyl)amino]heptanoate

: 1207984-53-9
ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

Guidance literature:: With hydrogen; Raney nickel; In ethanol; at 20 ℃; for 1h; under 760.051 Torr;

Reference yield:

: 7149-79-3
N-(3-chloro-4-methylphenyl)acetamide

: 1207984-53-9
ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C

2.1: methanol; sodium methylate / 5 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C

4.1: caesium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / ISOPROPYLAMIDE / 24.25 h / 20 - 150 °C / Inert atmosphere

5.1: hydrogen / Raney nickel / ethanol / 1 h / 20 °C / 760.05 Torr

With methanol; hydrogen; nitric acid; sodium methylate; acetic anhydride; sodium hydride; caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In ethanol; ISOPROPYLAMIDE; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 7149-78-2
5-chloro-4-methyl-2-nitroacetanilide

: 1207984-53-9
ethyl 7-[(2-amino-5-cyclopropyl-4-methylphenyl)amino]heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; sodium methylate / 5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: caesium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / ISOPROPYLAMIDE / 24.25 h / 20 - 150 °C / Inert atmosphere

4.1: hydrogen / Raney nickel / ethanol / 1 h / 20 °C / 760.05 Torr

With methanol; hydrogen; sodium methylate; sodium hydride; caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In ethanol; ISOPROPYLAMIDE; N,N-dimethyl-formamide;