2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

Base Information

Chemical Name:2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate
CAS No.:677031-70-8
Molecular Formula:C₄₄H₅₆O₂₇S₂
Molecular Weight:1081.04
Hs Code.:

2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

Synonyms:2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

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Chemical Property of 2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

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Technology Process of 2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

There total 4 articles about 2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 76821-27-7,78853-86-8,104932-59-4,106034-47-3,60438-67-7
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-bromide

: 1887-29-2
sodium phenylthiosulfonate

: 677031-70-8
2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; In acetonitrile; at 70 ℃; for 2h;
DOI:10.1039/b306990g

Reference yield: 62.0%

: 76821-27-7,78853-86-8,104932-59-4,106034-47-3,60438-67-7
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-α-D-glucopyranosyl-bromide

: 515-42-4
sodium phenylsulfonate

: 677031-70-8
2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; In acetonitrile; at 70 ℃; for 2h;

Reference yield:

: 76821-26-6
maltotriose peracetate

: 677031-70-8
2,3,6-tri-O-acetyl-4-O-(2,3,6-tri-D-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl)-β-D-glucopyranosyl phenylthiosulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / hydrogen bromide / CH₂Cl₂; acetic acid / 0.5 h / 20 °C

2: 68 percent / tetrabutylammonium iodide / acetonitrile / 2 h / 70 °C

With hydrogen bromide; tetra-(n-butyl)ammonium iodide; In dichloromethane; acetic acid; acetonitrile;
DOI:10.1039/b306990g