C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

Base Information

Chemical Name:C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2
CAS No.:922495-46-3
Molecular Formula:C₃₁H₂₀F₂N₄O
Molecular Weight:502.523
Hs Code.:

C<sub>5</sub>H<sub>4</sub>NC<sub>6</sub>H<sub>4</sub>C<sub>2</sub>ON<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>F)2

Synonyms:C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

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Chemical Property of C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

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Technology Process of C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

There total 7 articles about C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 922495-43-0
C₂₆H₁₆BrF₂N₃O

: 17997-47-6
2-tri-n-butylstannylpyridine

: 922495-46-3
C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 50h; Inert atmosphere;
DOI:10.1016/j.dyepig.2010.08.001

Reference yield:

: 922495-39-4
4-cyanophenyl-di(4-fluorophenyl)amine

: 922495-46-3
C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 90 h / Inert atmosphere; Reflux

2: pyridine / 48 h / Inert atmosphere; Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 50 h / 110 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; ammonium chloride; In N,N-dimethyl-formamide; toluene; 3: Stille coupling;
DOI:10.1016/j.dyepig.2010.08.001

Reference yield:

: 922495-38-3
4-(N,N-di(4-fluorophenyl)amino)benzaldehyde

: 922495-46-3
C₅H₄NC₆H₄C₂ON₂C₆H₄N(C₆H₄F)2

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; hydroxylamine hydrochloride; acetic acid / N,N-dimethyl-formamide / 9 h / 130 °C / Inert atmosphere

2: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 90 h / Inert atmosphere; Reflux

3: pyridine / 48 h / Inert atmosphere; Reflux

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 50 h / 110 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; hydroxylamine hydrochloride; ammonium chloride; acetic acid; In N,N-dimethyl-formamide; toluene; 4: Stille coupling;
DOI:10.1016/j.dyepig.2010.08.001