C₈₃H₈₈O₁₇

Base Information

• Chemical Name: C₈₃H₈₈O₁₇
• CAS No.: 1426575-87-2
• Molecular Formula: C₈₃H₈₈O₁₇
• Molecular Weight: 1357.6
• Mol file: 1426575-87-2.mol

Synonyms:C₈₃H₈₈O₁₇

Chemical Property of C₈₃H₈₈O₁₇

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₈₃H₈₈O₁₇

There total 1 articles about C₈₃H₈₈O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl 2-O-(4-methoxybenzyl)-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside (1235579-84-6) + methyl 2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-D-glucopyranoside (19474-56-7) → C83H88O17 (1426575-86-1) + C83H88O17 (1426575-87-2)

Guidance literature:

phenyl 2-O-(4-methoxybenzyl)-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside; methyl 2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-D-glucopyranoside; With N-iodo-succinimide; In diethyl ether; dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

With trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -45 ℃; Overall yield = 59 %; Overall yield = 17.5 mg; Inert atmosphere;

DOI:10.1016/j.carres.2012.12.015

upstream raw materials:

phenyl 2-O-(4-methoxybenzyl)-3-O-benzyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

methyl 2,3,6-tri-O-benzyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-D-glucopyranoside