3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE)

Base Information

Chemical Name:3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE)
CAS No.:1212092-04-0
Molecular Formula:C₁₆H₁₅NO₄
Molecular Weight:285.299
Hs Code.:
Mol file:1212092-04-0.mol

Synonyms:3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0*1,5*]dec-8-ene-6-carboxylic acid

Suppliers and Price of 3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE)

There total 6 articles about 3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0~1,5~]dec-8-ene-6-carboxylic acid(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-31-6
maleic anhydride

: 4439-53-6
N-benzyl(furan-2-ylmethyl)amine

: 1212092-04-0
3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0*1,5*]dec-8-ene-6-carboxylic acid

Guidance literature:: In toluene; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.9b00642

Reference yield:

: 100-46-9
benzylamine

: 1212092-04-0
3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0*1,5*]dec-8-ene-6-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 4 h / Reflux

2: sodium cyanoborohydride; trifluoroacetic acid / methanol / 2.5 h / 0 - 20 °C

3: toluene / 5 h / Reflux

With sodium cyanoborohydride; trifluoroacetic acid; In methanol; toluene; benzene; 3: Diels-Alder reaction;
DOI:10.1021/jm3002839

Reference yield:

: 98-01-1
furfural

: 1212092-04-0
3-benzyl-4-oxo-10-oxa-3-azatricyclo[5.2.1.0*1,5*]dec-8-ene-6-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 4 h / Reflux

2: sodium cyanoborohydride; trifluoroacetic acid / methanol / 2.5 h / 0 - 20 °C

3: toluene / 5 h / Reflux

With sodium cyanoborohydride; trifluoroacetic acid; In methanol; toluene; benzene; 3: Diels-Alder reaction;
DOI:10.1021/jm3002839