N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

Base Information

Chemical Name:N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride
CAS No.:770747-16-5
Molecular Formula:C₃₀H₃₄ClCrN₂O₄
Molecular Weight:574.06
Hs Code.:

Synonyms:N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

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Chemical Property of N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

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Technology Process of N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

There total 2 articles about N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: chromium dichloride

: 770747-21-2
N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediimine

: 770747-16-5
N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

: 6,6'-(1,2,3,4-tetrahydroquinoxaline-2,3-diyl)bis(2-(tert-butyl)-4-methoxyphenol)

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1039/d0cc01192d

Reference yield:

: 121-00-6,1341-82-8
3-tert-Butyl-4-hydroxyanisole

: 770747-16-5
N,N'-bis(3-tert-butyl-5-methoxysalicylidene)-1,2-phenylenediamino chromium(III) chloride

: 6,6'-(1,2,3,4-tetrahydroquinoxaline-2,3-diyl)bis(2-(tert-butyl)-4-methoxyphenol)

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium chloride; triethylamine / tetrahydrofuran / 16 h / Reflux

2: methanol / 16 h / Reflux

3: tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

With triethylamine; magnesium chloride; In tetrahydrofuran; methanol;
DOI:10.1039/d0cc01192d