[1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Base Information

• Chemical Name: [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine
• CAS No.: 274917-26-9
• Molecular Formula: C₁₅H₁₃N₅O₂
• Molecular Weight: 295.301
• Mol file: 274917-26-9.mol

Synonyms:[1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Chemical Property of [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

There total 1 articles about [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrobenzaldehdye (555-16-8) + 1-(o-azidophenyl)ethylamine (146954-07-6) → [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (274917-26-9)

Guidance literature:

With magnesium sulfate; In diethyl ether; at 25 ℃; for 12h;

DOI:10.1021/jo991826q

Reference yield: 77.0%

phenylethylketene (20452-67-9) + [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (274917-26-9) → (1SR,2RS,8SR)-1,2-cis-1,8-trans-2-ethyl-8-methyl-1-(4-nitrophenyl)-2-phenyl-1,2-dihydroazeto[2,1-b]quinazoline

Guidance literature:

[1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine; With trimethylphosphane; In toluene; at 25 ℃;

phenylethylketene; In toluene; at 25 ℃;

DOI:10.1016/j.tetasy.2003.11.025

Reference yield: 75.0%

methyl phenyl ketene (3156-07-8) + [1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (274917-26-9) → (1SR,2RS,8SR)-1,2-cis-1,8-trans-2,8-dimethyl-1-(4-nitrophenyl)-2-phenyl-1,2-dihydroazeto[2,1-b]quinazoline

Guidance literature:

[1-(2-Azido-phenyl)-ethyl]-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine; With trimethylphosphane; In toluene; at 25 ℃;

methyl phenyl ketene; In toluene; at 25 ℃;

DOI:10.1016/j.tetasy.2003.11.025

upstream raw materials:

4-nitrobenzaldehdye

1-(o-azidophenyl)ethylamine

Downstream raw materials:

Diphenylvinylidene-[2-(1-{[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amino}-ethyl)-phenyl]-amine