Technology Process of C30H39F3N2O4SSi
There total 3 articles about C30H39F3N2O4SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver(I) acetate; palladium diacetate;
In
toluene;
at 100 ℃;
Inert atmosphere;
DOI:10.1021/ol4020877
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere
1.2: 3 h / -78 °C / Inert atmosphere
2.1: palladium diacetate; silver(I) acetate / toluene / 100 °C / Inert atmosphere
With
n-butyllithium; silver(I) acetate; palladium diacetate;
In
tetrahydrofuran; toluene;
DOI:10.1021/ol4020877
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 4 h / -78 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere
2.2: 3 h / -78 °C / Inert atmosphere
3.1: palladium diacetate; silver(I) acetate / toluene / 100 °C / Inert atmosphere
With
n-butyllithium; silver(I) acetate; palladium diacetate; triethylamine;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol4020877
