(1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

Base Information

Chemical Name:(1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid
CAS No.:1091619-79-2
Molecular Formula:C₂₅H₂₂N₂O₆S
Molecular Weight:478.525
Hs Code.:

Synonyms:(1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

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Technology Process of (1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

There total 2 articles about (1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 370065-09-1
4-(4-methoxyphenoxy)benzenesulfonyl chloride

: C₃₁H₂₄ClN₂O₂Pol

: 1091619-79-2
(1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

Guidance literature:: C₃₁H₂₄ClN₂O₂Pol; With dmap; In tetrahydrofuran; for 1h; 2-chlorotrityl resin

4-(4-methoxyphenoxy)benzenesulfonyl chloride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 18h;

With acetic acid; In tetrahydrofuran; dichloromethane; 2,2,2-trifluoroethanol;

Reference yield:

: C₄₄H₃₄ClN₂O₆PolS

: 1091619-79-2
(1RS)-2-(4''-methoxy-4'-phenoxybenzenesulfonyl)-1,2,3,4-tetrahydro-norarmano-1-carboxylic acid

Guidance literature:: With 2,2,2-trifluoroethanol; acetic acid; In dichloromethane; at 20 ℃; for 1h; 2-chlorotrityl resin
DOI:10.1002/cmdc.201800237