phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

Base Information

Chemical Name:phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate
CAS No.:811788-87-1
Molecular Formula:C₂₃H₂₇FN₂O₆
Molecular Weight:446.476
Hs Code.:

Synonyms:phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

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Chemical Property of phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

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Technology Process of phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

There total 1 articles about phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 811788-86-0
benzyl 4-amino-3-fluorobenzoate

: 40856-59-5,132957-40-5
tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate

: 811788-87-1
phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

Guidance literature:: benzyl 4-amino-3-fluorobenzoate; With trimethylaluminum; In n-heptane; dichloromethane; at 20 - 30 ℃; for 1.08333h;

tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate; In n-heptane; dichloromethane; for 20h;

Reference yield:

: 811788-87-1
phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

: phenylmethyl 4-[3-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-oxo-1-pyrrolidinyl]3-fluorobenzoate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate; In tetrahydrofuran; at 5 - 20 ℃; for 20.5h;

Reference yield:

: 811788-87-1
phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate

: 811788-88-2
phenylmethyl 4-[(3S)-3-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-oxo-1-pyrrolidinyl]-3-fluorobenzoate

Guidance literature:: phenylmethyl 4-[(N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-homoseryl)amino]-3-fluorobenzoate; With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 5 - 20 ℃; for 20.5h;

With citric acid; In tetrahydrofuran; water;