N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide

Base Information

• Chemical Name: N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide
• CAS No.: 1005326-41-9
• Molecular Formula: C₁₉H₁₉Cl₃N₄O
• Molecular Weight: 425.745

Synonyms:N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide

Chemical Property of N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide

Chemical Property:

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Technology Process of N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide

There total 1 articles about N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N-(4-chloro-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl)-2,2-dimethylpropanamide (1005326-34-0) + 3,5-dichlorobenzyl bromide (7778-01-0) → N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide (1005326-41-9)

Guidance literature:

N-(4-chloro-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl)-2,2-dimethylpropanamide; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

3,5-dichlorobenzyl bromide; In N,N-dimethyl-formamide; at 0 ℃; for 3h; Further stages.;

DOI:10.1021/jm701052u

Reference yield:

N-[4-chloro-5-(3,5-dichlorobenzyl)-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl]-2,2-dimethylpropanamide (1005326-41-9) → C14H12Cl2N4O (1005326-18-0)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; for 24h; Heating;

DOI:10.1021/jm701052u

upstream raw materials:

N-(4-chloro-6-methyl-5H-pyrrolo[3,2-d]pyrimidin-2-yl)-2,2-dimethylpropanamide

3,5-dichlorobenzyl bromide

Downstream raw materials:

C₁₄H₁₂Cl₂N₄O

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