(4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester

Base Information

• Chemical Name: (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester
• CAS No.: 76284-32-7
• Molecular Formula: C₁₄H₁₂ClN₃O₄S
• Molecular Weight: 353.786

Synonyms:(4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester

Chemical Property of (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester

Chemical Property:

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Technology Process of (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester

There total 1 articles about (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-benzyloxycarbonylamino)thiazol-4-yl-2-(Z)-methoxyiminoacetic acid (76284-36-1) → (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester (76284-32-7)

Guidance literature:

With phosphorus pentachloride; In tetrahydrofuran; pyridine; dichloromethane; for 1h;

DOI:10.1248/cpb.28.1563

Reference yield: 80.0%

(6R,7S)-7-Amino-3-methyl-8-oxo-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester (69885-03-6,73910-38-0) + (4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester (76284-32-7) → (6R,7S)-7-{2-[2-(Cyclohexa-2,4-dienylmethoxycarbonylamino)-thiazol-4-yl]-2-[(Z)-methoxyimino]-acetylamino}-3-methyl-8-oxo-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester

Guidance literature:

DOI:10.1248/cpb.28.1563

Reference yield: 77.0%

(4-{Chlorocarbonyl-[(Z)-methoxyimino]-methyl}-thiazol-2-yl)-carbamic acid benzyl ester (76284-32-7) + (6R,7S)-7-Amino-3-(1-methyl-1H-tetrazol-5-ylsulfanylmethyl)-8-oxo-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzyl ester (62284-41-7,73951-73-2) → benzyl 7β-<2-(2-benzyloxycarbonylamino)thiazole-4-yl-2-(Z)-methoxyimino>acetylamino-3-(1-methyl-1H-tetrazol-5-yl)thiomethyl-1-carba-1-dethia-3-cephem-4-carboxylate

Guidance literature:

In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.583333h;

DOI:10.1248/cpb.28.1563

upstream raw materials:

2-(2-benzyloxycarbonylamino)thiazol-4-yl-2-(Z)-methoxyiminoacetic acid

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