N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

Base Information

Chemical Name:N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide
CAS No.:886754-88-7
Molecular Formula:C₂₀H₂₄N₄O₂
Molecular Weight:352.436
Hs Code.:

Synonyms:N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

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Technology Process of N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

There total 3 articles about N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 886754-84-3
1-phenyl-3-(9,9,9a-trimethyl-2-oxo-2,3,9,9a-tetrahydro-1H-imidazo[1,2-a]indol-1-yl)urea

: 886754-88-7
N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 70 ℃;
DOI:10.1016/j.tet.2006.01.054

Reference yield:

: 401834-53-5
1-amino-1,2,3,9a-tetrahydro-9,9,9a-trimethylimidazolo[1,2-a]indol-2(9H)-one

: 886754-88-7
N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / toluene / 2 h / 80 °C

2: 71 percent / sodium borohydride / ethanol / 70 °C

With sodium tetrahydroborate; In ethanol; toluene;
DOI:10.1016/j.tet.2006.01.054

Reference yield:

: 90907-07-6
1-carbamoylmethyl-2,3,3-trimethyl-3H-indolinium chloride

: 886754-88-7
N-phenyl-2-[(2,3,3-trimethyl-2,3-dihydro-1H-indol-1-yl)acetyl]hydrazinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / hydrazine dihydrate / 0.5 h / 70 °C

2: 38 percent / toluene / 2 h / 80 °C

3: 71 percent / sodium borohydride / ethanol / 70 °C

With sodium tetrahydroborate; hydrazine hydrate; In ethanol; toluene;
DOI:10.1016/j.tet.2006.01.054