N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

Base Information

Chemical Name:N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine
CAS No.:153576-83-1
Molecular Formula:C₂₇H₃₁NO₅S
Molecular Weight:481.613
Hs Code.:

Synonyms:N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

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Chemical Property of N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

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Technology Process of N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

There total 5 articles about N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 153576-82-0
N-carbethoxy-N-(2-phenylthio-2-phenylethyl)-3,4-dimethoxyphenylethylamine

: 153576-83-1
N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

Guidance literature:: With sodium periodate; In methanol; for 48h; Ambient temperature;
DOI:10.1080/00397919308012581

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 153576-83-1
N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 1 h / Heating

2: 10percent aq. NaOH / diethyl ether / 1 h / Ambient temperature

3: 82 percent / NaBH₄, glacial acetic acid / tetrahydrofuran / 18 h / Heating

4: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

5: 100 percent / sodium periodate / methanol / 48 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; thionyl chloride; acetic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1080/00397919308012581

Reference yield:

: 10313-60-7
3,4-dimethoxyphenylacetyl chloride

: 153576-83-1
N-carbethoxy-N-(2-phenylsulfinyl-2-phenylethyl)-3,4-dimethoxyphenylethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 10percent aq. NaOH / diethyl ether / 1 h / Ambient temperature

2: 82 percent / NaBH₄, glacial acetic acid / tetrahydrofuran / 18 h / Heating

3: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 100 percent / sodium periodate / methanol / 48 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; acetic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1080/00397919308012581