1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

Base Information

Chemical Name:1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone
CAS No.:442128-47-4
Molecular Formula:C₂₃H₂₂N₂O₃
Molecular Weight:374.439
Hs Code.:

Synonyms:1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

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Chemical Property of 1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

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Technology Process of 1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

There total 1 articles about 1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 97674-02-7
tributyl(1-ethoxyvinyl)stannane

: 442128-24-7
1-[2-(4-benzyloxyphenyl)-6-chloro-pyrimidin-4-yl]-ethyl ketone

: 442128-47-4
1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

Guidance literature:: bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1021/jo702495u

Reference yield:

: 442128-47-4
1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

: C₈₃H₅₄N₁₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 4 h / Heating

2: aq. HCl / acetone / 20 °C

3: 80 percent / KOH / pyridine / 3 h / Heating

With hydrogenchloride; potassium hydroxide; potassium hydroxide; In pyridine; ethanol; acetone;
DOI:10.1002/1521-3773(20020402)41:7<1195::AID-ANIE1195>3.0.CO;2-L

Reference yield:

: 442128-47-4
1-[2-(4-benzyloxyphenyl)-6-(1-ethoxyvinyl)-pyrimidin-4-yl]-ethyl ketone

: 442128-55-4
1-[2-(4-benzyloxyphenyl)-6-[1,8]naphthyridin-2-yl-pyrimidin-4-yl]ethyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 4 h / Heating

2: aq. HCl / acetone / 20 °C

With hydrogenchloride; potassium hydroxide; In ethanol; acetone;
DOI:10.1002/1521-3773(20020402)41:7<1195::AID-ANIE1195>3.0.CO;2-L