N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

Base Information

Chemical Name:N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide
CAS No.:69909-92-8
Molecular Formula:C₂₂H₁₈N₄S
Molecular Weight:370.478
Hs Code.:

Synonyms:N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

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Technology Process of N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

There total 5 articles about N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 20800-34-4
1-Phenyl-3-[1-phenyl-1-phenylamino-meth-(Z)-ylidene]-thiourea

: 75-05-8,26809-02-9
acetonitrile

: 69909-92-8
N-(3-methyl-4-phenyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

Guidance literature:: With [bis(acetoxy)iodo]benzene; In neat (no solvent); at 50 ℃; for 0.0333333h;
DOI:10.1002/adsc.201800353

Reference yield:

: N-phenylbenzamidine

: (1E,NZ)-N-(4-benzyl-3-methyl-1,2,4-thiadiazol-5(4H)-ylidene)-N'-phenylbenzimidamide

: 69909-92-8
C₂₂H₁₈N₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-ethane / 16 h / 55 °C

2: bromine / dichloromethane; ethyl acetate / 20 °C

3: triethylamine / acetonitrile / 0.5 h / Reflux

With bromine; triethylamine; In dichloromethane; ethyl acetate; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.chembiol.2018.04.010