[Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]

Base Information

• Chemical Name: [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]
• CAS No.: 1019651-33-2
• Molecular Formula: C₅₆H₄₉Fe₂NO₂P₄S₂
• Molecular Weight: 1067.73

Synonyms:[Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]

Chemical Property of [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]

Chemical Property:

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Technology Process of [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]

There total 3 articles about [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

Fe2(S2(CH2)2NH)(CO)4(cis-1,2-bis(diphenylphosphino)ethylene) (932722-51-5,932706-72-4) + cis-1,2-bis-(diphenylphosphino)ethene (983-80-2) → [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)] (1019651-33-2)

Guidance literature:

In toluene; for 24h; Schlenk technique; Irradiation;

DOI:10.1021/ja309216v

Reference yield:

[Fe2(CO)2(μ-hydride)(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]B(C6H3(CF3)2)4 → [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)] (1019651-33-2)

Guidance literature:

With triethylamine; In not given; treatment of iron compd. with triethylamine at room temp.;

DOI:10.1021/ja8057666

Reference yield:

[Fe2H(CO)(μ-CO)(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]B(C6H3(CF3)2)4 (1019651-39-8) → [Fe2(CO)2(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)] (1019651-33-2)

Guidance literature:

With P(CH₂CH₂CH₂CH₃)3; In dichloromethane-d2; treatment of iron compd. with phosphine deriv. at -90°C;

DOI:10.1021/ja8057666

upstream raw materials:

[Fe2H(CO)(μ-CO)(cis-1,2-bis(diphenylphosphino)ethylene)2(μ-2-azapropane-1,3-dithiolate)]B(C6H3(CF3)2)4

Fe₂(S₂(CH₂)2NH)(CO)4(cis-1,2-bis(diphenylphosphino)ethylene)

cis-1,2-bis-(diphenylphosphino)ethene

Downstream raw materials:

Fe2(μ-H)(SCH2NHCH2S)(CO)2(cis-1,2-bis(diphenylphosphino)ethene)](1+)

C₅₆H₅₀Fe₂NO₂P₄S₂⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-)

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