N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

Base Information

Chemical Name:N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt
CAS No.:122923-55-1
Molecular Formula:C₂₈H₃₇N₄O₉P*2Na
Molecular Weight:650.576
Hs Code.:

Synonyms:N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

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Chemical Property of N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

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Technology Process of N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

There total 3 articles about N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.71%

: 122900-07-6
N-(diethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine methyl ester

: 122923-55-1
N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

Guidance literature:: With sodium hydroxide; In ethanol; for 19h;
DOI:10.1021/jm00163a044

Reference yield:

: 122900-74-7
(2S,3S)-2-(Diethoxy-phosphorylamino)-3-methyl-pentanoic acid benzyl ester

: 122923-55-1
N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂ / 10percent Pd/C / methanol / 760 Torr

2: 70 percent / DCC / dimethylformamide / 0 °C / overnight

3: 0.71 percent / aq. NaOH / ethanol / 19 h

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00163a044

Reference yield:

: 122899-90-5
N-(diethylphosphoryl)-L-isoleucine

: 122923-55-1
N-(ethylphosphoryl)-L-isoleucyl-O-<<(N-benzylamino)carbonyl>methyl>-L-tyrosylglycine disodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / DCC / dimethylformamide / 0 °C / overnight

2: 0.71 percent / aq. NaOH / ethanol / 19 h

With sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00163a044