(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Base Information

Chemical Name:(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene
CAS No.:109308-29-4
Molecular Formula:C₁₇H₂₂S
Molecular Weight:258.428
Hs Code.:

Synonyms:(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

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Chemical Property of (3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

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Technology Process of (3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

There total 9 articles about (3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110950-00-0
(Z)-3-<(phenylthio)methyl>-8-methyl-1,3,8-nonatriene

: 109308-30-7
(3aS,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

: 109308-29-4
(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: With DBTH; In benzene; at 200 - 220 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Further solvent: N,N-dimethylaniline;
DOI:10.1016/S0040-4039(00)87789-8

Reference yield:

: 109432-19-1
(Z)-2-<(phenylthio)methyl>-2-nonen-1-ol

: 109308-29-4
(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridinium dichromate (PDC) / dimethylformamide / 2 h

2: dimethylsulfoxide / 6 h

3: 2,5-di-tert-butylhydroquinone (DTBH) / various solvent(s) / 4 h / Heating

With dipyridinium dichromate; 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo00228a040

Reference yield:

: 109307-70-2
(Z)-2-<(phenylthio)methyl>-2-nonenal

: 109308-29-4
(3aR,7aS)-3a-Methyl-7-phenylsulfanylmethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide / 6 h

2: 2,5-di-tert-butylhydroquinone (DTBH) / various solvent(s) / 4 h / Heating

With 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; In dimethyl sulfoxide;
DOI:10.1021/jo00228a040