Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH))

Base Information

• Chemical Name: Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH))
• CAS No.: 98586-59-5
• Molecular Formula: C₃₁H₂₅NaO₃P₂W
• Molecular Weight: 714.325

Synonyms:Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH))

Chemical Property of Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH))

Chemical Property:

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Technology Process of Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH))

There total 1 articles about Na⁽¹⁺⁾*(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)^(1-)=Na((OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium acetylide (115570-70-2,1066-26-8) + fac-W(CO)3(bis(diphenylphoshino)ethane)(acetone) (84411-66-5,87900-84-3) → Na(1+)*(OC)3((C6H5)2PCH2CH2P(C6H5)2)W(CCH)(1-)=Na((OC)3((C6H5)2PCH2CH2P(C6H5)2)W(CCH)) (98586-59-5)

Guidance literature:

In tetrahydrofuran;

Reference yield: 53.0%

Na(1+)*(OC)3((C6H5)2PCH2CH2P(C6H5)2)W(CCH)(1-)=Na((OC)3((C6H5)2PCH2CH2P(C6H5)2)W(CCH)) (98586-59-5) → (OC)3((C6H5)2PCH2CH2P(C6H5)2)W(CCH2) (98586-72-2)

Guidance literature:

With HBF₄; In dichloromethane; aq. HBF4 was added to a slurry of W-complex in CH2Cl2 at 0°C, mixt. was kept at 0°C; dried over MgSO4, filtered, filtrate was concd., hexane added, ppt. wascollected;

upstream raw materials:

sodium acetylide

fac-W(CO)3(bis(diphenylphoshino)ethane)(acetone)

Downstream raw materials:

(OC)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂)

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