5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone

Base Information

Chemical Name:5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
CAS No.:157666-07-4
Molecular Formula:C₉H₁₃BrO₄
Molecular Weight:265.104
Hs Code.:
Mol file:157666-07-4.mol

Synonyms:Furo[3,4-d]-1,3-dioxole,D-ribonic acid deriv.

Suppliers and Price of 5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
100 mg
$ 124.00

Biosynth Carbosynth
5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
50 mg
$ 71.00

Biosynth Carbosynth
5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
250 mg
$ 247.50

Biosynth Carbosynth
5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
500 mg
$ 430.00

Biosynth Carbosynth
5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone
1 g
$ 750.00

AK Scientific
(3Ar,6S,6aR)-6-(bromomethyl)-2,2,3a-trimethyl-6,6a-dihydrofuro[3,4-d][1,3]dioxol-4-one
1g
$ 1062.00

AK Scientific
(3Ar,6S,6aR)-6-(bromomethyl)-2,2,3a-trimethyl-6,6a-dihydrofuro[3,4-d][1,3]dioxol-4-one
500mg
$ 630.00

AK Scientific
(3Ar,6S,6aR)-6-(bromomethyl)-2,2,3a-trimethyl-6,6a-dihydrofuro[3,4-d][1,3]dioxol-4-one
250mg
$ 384.00

AK Scientific
(3Ar,6S,6aR)-6-(bromomethyl)-2,2,3a-trimethyl-6,6a-dihydrofuro[3,4-d][1,3]dioxol-4-one
100mg
$ 217.00

AK Scientific
(3Ar,6S,6aR)-6-(bromomethyl)-2,2,3a-trimethyl-6,6a-dihydrofuro[3,4-d][1,3]dioxol-4-one
50mg
$ 145.00

Total 6 raw suppliers

Chemical Property of 5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone

Chemical Property:

PSA：44.76000
Density:1.472
LogP:1.21690

Purity/Quality:

99% ^*data from raw suppliers

5-Bromo-5-deoxy-2-c-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone

There total 1 articles about 5-Bromo-5-deoxy-2-C-methyl-2,3-O-(1-methylethylidene)-D-ribonic-gamma-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 23709-41-3
2-methyl-2,3-O-(1-methylethylidene)-D-ribonic acid γ-lactone

: 157666-07-4
5-Bromo-2,3-O-isopropylidene-2-C-methyl-D-ribono-1,4-lactone

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; barium carbonate; In dichloromethane; for 0.5h; Heating;

Reference yield:

: 157666-07-4
5-Bromo-2,3-O-isopropylidene-2-C-methyl-D-ribono-1,4-lactone

: (2R,3R)-2,3-Dihydroxy-2,3-O-isopropylidene-2-methyl-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Zn / ethanol / 2 h / Heating

2: 94.3 percent / H₂ / Pd/C / ethyl acetate / 12 h / Ambient temperature

With hydrogen; zinc; palladium on activated charcoal; In ethanol; ethyl acetate;