N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

Base Information

Chemical Name:N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide
CAS No.:1261241-46-6
Molecular Formula:C₃₄H₄₃NO₇
Molecular Weight:577.718
Hs Code.:

Synonyms:N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

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Chemical Property of N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

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Technology Process of N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

There total 5 articles about N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 57079-01-3
11-(2,5-dioxopyrrol-1-yl)undecanoic acid

: 33905-64-5
4-hydroxyphenyl 4'-n-hexyloxybenzoate

: 1261241-46-6
N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In chloroform; at -9.96 - 20 ℃; for 2.5h;
DOI:10.1002/pola.24463

Reference yield:

: N-(10-carboxy-n-decyl)maleamic acid

: 1261241-46-6
N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 9 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / chloroform / 2.5 h / -9.96 - 20 °C

With dmap; dicyclohexyl-carbodiimide; In chloroform; acetic acid;
DOI:10.1002/pola.24463

Reference yield:

: 111-25-1
1-bromo-hexane

: 1261241-46-6
N-[10-((4-(((4'-n-hexyloxy)benzoyl)oxy)phenoxy)carbonyl)-n-decyl]maleimide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; potassium hydroxide / ethanol; water / Inert atmosphere; Reflux

2: sulfuric acid; boric acid / toluene / 7 h / Inert atmosphere; Reflux

3: dmap; dicyclohexyl-carbodiimide / chloroform / 2.5 h / -9.96 - 20 °C

With dmap; sulfuric acid; boric acid; dicyclohexyl-carbodiimide; potassium iodide; potassium hydroxide; In ethanol; chloroform; water; toluene;
DOI:10.1002/pola.24463