(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

Base Information

Chemical Name:(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril
CAS No.:95853-79-5
Molecular Formula:C₁₈H₂₆N₂O₂
Molecular Weight:302.417
Hs Code.:

Synonyms:(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

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Chemical Property of (2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

Chemical Property:

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Technology Process of (2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

There total 1 articles about (2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 143-33-9,25596-52-5
sodium cyanide

: 590-86-3
isovaleraldehyde

: 35019-66-0
(4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine

: 95853-79-5
(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

: 95853-78-4
(2R)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

Guidance literature:: In ethylene glycol; for 1h; Yields of byproduct given; Ambient temperature;

Reference yield: 78.0%

: 95853-79-5
(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

: 95853-80-8
(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Guidance literature:: With hydrogenchloride; In water; 1.) 1 h, -13 deg C, 2.) 1h, 0 deg C, 3.) 1 h, room temperature, 4.) 4 h, 60 deg C;

Reference yield:

: 95853-79-5
(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 12 N HCl / H₂O / 1.) 1 h, -13 deg C, 2.) 1h, 0 deg C, 3.) 1 h, room temperature, 4.) 4 h, 60 deg C

2: 67 percent / orthoperiodic acid, 2 N NH₃ / H₂O / 14 h / Ambient temperature

With hydrogenchloride; ammonium hydroxide; periodic acid; In water;