(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

Base Information

Chemical Name:(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin
CAS No.:123169-16-4
Molecular Formula:C₂₄H₃₉F₂N₃O₇Si₂
Molecular Weight:575.757
Hs Code.:

(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta<f>-1,3,5,2,4-trioxadisilocin

Synonyms:(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

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Chemical Property of (+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

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Technology Process of (+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

There total 2 articles about (+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 110880-87-0
(+/-)-(6aα,8β,9aβ)-8-<2,4-dinitrophenyl)amino>hexahydro-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin-9-one

: 123169-16-4
(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 5 ℃; for 1h;
DOI:10.1021/jm00163a030

Reference yield:

: 110864-89-6
(1RS,8RS,10RS,11SR)-10-(2,4-dinitroanilino)-3,3,5,5-tetraisopropyl-2,4,6-trioxa-3,5-disilabicyclo<6.3.0>undecan-11-ol

: 123169-16-4
(+/-)-(6aα,8β,9aβ)-9,9-difluorohexahydro-8-<2,4-dinitrophenyl)amino>-2,2,4,4-tetrakis(1-methylethyl)cyclopenta-1,3,5,2,4-trioxadisilocin

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / 1.) dicyclohexylcarbodiimide, H₃PO₄, 2.) ethyl acetate, oxalic acid / 1.) DMSO, RT, 3.5 h, 2.) methanol, RT, 5 min

2: 25 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 1 h / 5 °C

With diethylamino-sulfur trifluoride; phosphoric acid; oxalic acid; ethyl acetate; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00163a030