N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline

Base Information

• Chemical Name: N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline
• CAS No.: 1364952-72-6
• Molecular Formula: C₂₃H₁₆Br₂F₂N₂O
• Molecular Weight: 534.198

Synonyms:N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline

Chemical Property of N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline

Chemical Property:

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Technology Process of N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline

There total 1 articles about N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-bromo-2,2-difluoro-N-(4-methoxyphenyl)acetimidoyl chloride + 5-bromo-2-phenylindole (83515-06-4) → N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline (1364952-72-6)

Guidance literature:

5-bromo-2-phenylindole; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 1.33333h; Inert atmosphere;

2-bromo-2,2-difluoro-N-(4-methoxyphenyl)acetimidoyl chloride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/c2cc30207a

Reference yield: 90.0%

N-(2-bromo-1-(5-bromo-2-phenyl-1H-indol-1-yl)-2,2-difluoroethylidene)-4-methoxyaniline (1364952-72-6) → N-(10-bromo-5,5-difluoroindolo[2,1-a]isoquinolin-6(5H)-ylidene)-4-methoxyaniline (1364953-45-6)

Guidance literature:

With Wilkinson's catalyst; silver carbonate; In 1,4-dioxane; at 100 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2cc30207a

upstream raw materials:

5-bromo-2-phenylindole

Downstream raw materials:

N-(10-bromo-5,5-difluoroindolo[2,1-a]isoquinolin-6(5H)-ylidene)-4-methoxyaniline

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