2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole

Base Information

Chemical Name:2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole
CAS No.:149894-30-4
Molecular Formula:C₁₄H₁₃F₅N₂O
Molecular Weight:320.262
Hs Code.:

Synonyms:2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole

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Technology Process of 2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole

There total 1 articles about 2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 149894-30-4
2-(2',4'-difluorophenyl)-3-trifluoromethyl-3-hydroxy-3,3a,4,5,6,7-hexahydroindazole

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / MeONa / diethyl ether / 18 h / Ambient temperature

2: 1.) pyrrolidine, 3 Angstroem molecular sieve / 1.) THF, 0 deg C, 30 min, 2.) THF, to r.t., overnight

With pyrrolidine; 3 A molecular sieve; sodium methylate; In diethyl ether;
DOI:10.1002/mrc.1260310402