5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate

Base Information

• Chemical Name: 5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate
• CAS No.: 1197286-22-8
• Molecular Formula: C₇H₈O₃S*C₁₃H₁₃N₃
• Molecular Weight: 383.471

Synonyms:5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate

Chemical Property of 5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate

Chemical Property:

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Technology Process of 5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate

There total 1 articles about 5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2⁽¹¹⁾.3.5,7,9-pentaene tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.84%

varenicline (249296-44-4) + toluene-4-sulfonic acid (104-15-4) → 5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2(11).3.5,7,9-pentaene tosylate (1197286-22-8)

Guidance literature:

In isopropyl alcohol; at 0 - 75 ℃; for 1.25h; Product distribution / selectivity;

Reference yield: 95.06%

5,8,14-triazatetracyclo[10.3.1.0(2,11).0(4,9)]hexadeca-2(11).3.5,7,9-pentaene tosylate (1197286-22-8) → varenicline (249296-44-4)

Guidance literature:

With ammonia; In water; at 20 - 30 ℃; pH=9 - 10; Product distribution / selectivity;

upstream raw materials:

varenicline

toluene-4-sulfonic acid

Downstream raw materials:

varenicline

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