2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

Base Information

Chemical Name:2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester
CAS No.:479065-39-9
Molecular Formula:C₁₅H₂₀N₂O₆
Molecular Weight:324.334
Hs Code.:

Synonyms:2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

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Chemical Property of 2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

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Technology Process of 2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

There total 5 articles about 2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 479065-38-8
2-(methoxyacetamido)-5-nitroterephthalic acid diethyl ester

: 479065-39-9
2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1.5h; under 2585.74 Torr;
DOI:10.1021/jm020285l

Reference yield:

: 610-29-7
2-nitroterephthalic acid

: 479065-39-9
2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 59 percent / H₂SO₄ / 24 h / Heating

2: 85 percent / H₂ / 5 percent Pd/C / ethanol / 4 h / 2585.74 Torr

3: 80 percent / pyridine / benzene / 2 h / 20 °C

4: 72 percent / red fuming nitric acid / 0.5 h

5: 82 percent / H₂ / 5 percent Pd/C / ethanol / 1.5 h / 2585.74 Torr

With pyridine; sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jm020285l

Reference yield:

: 27210-70-4
2-aminoterephthalic acid diethyl ester

: 479065-39-9
2-(methoxyacetamido)-5-aminoterephthalic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / benzene / 2 h / 20 °C

2: 72 percent / red fuming nitric acid / 0.5 h

3: 82 percent / H₂ / 5 percent Pd/C / ethanol / 1.5 h / 2585.74 Torr

With pyridine; hydrogen; nitric acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/jm020285l